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BROOKFIELD VISCOSITY AT 135C DEG C (Pa-s) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 34 0.40 0.05 0.15 12.7 36.0 0.40 0.05 0.13 11.6 32.9 0.01 0.03 3.0 8.4 3.0 8.4 159 160 40 0.22 0.02 0.06 9.0 25.6 0.22 0.02 0.05 8.4 23.7 0.01 0.03 4.3 12.1 4.2 11.9 161 162 48 0.40 0.03 0.10 8.5 24.0 0.40 0.04 0.11 9.9 28.0 0.01 0.03 2.9 8.1 2.8 8.1 163 164 72 0.22 0.03 0.10 15.4 43.6 0.22 0.03 0.09 15.3 43.3 0.01 0.03 4.3 12.2 4.3 12.2 165 166 83 2.11 0.22 0.62 10.3 29.2 2.12 0.20 0.56 9.3 26.3 0.06 0.17 2.8 8.0 2.8 8.0 167 168 121 0.51 0.04 0.12 8.0 22.7 0.51 0.04 0.11 7.9 22.4 0.02 0.05 3.2 9.0 3.2 9.1 169 170 132 0.41 0.03 0.09 7.8 22.2 0.41 0.03 0.09 7.6 21.4 0.01 0.03 2.2 6.2 2.2 6.2 171 172 151 0.32 0.02 0.07 7.2 20.3 0.32 0.02 0.06 6.5 18.5 0.01 0.02 2.4 6.8 2.4 6.8 173 174 165 0.32 0.04 0.11 11.9 33.8 0.26 0.04 0.10 13.8 39.0 0.02 0.05 5.0 14.3 6.1 17.2 175 176 169 1.47 0.09 0.25 5.9 16.8 1.46 0.08 0.23 5.6 15.9 0.03 0.09 2.1 6.0 2.1 6.0 177 178 180 0.23 0.02 0.05 7.4 20.8 0.23 0.02 0.05 7.8 21.9 0.01 0.02 3.4 9.7 3.4 9.7 179 180 177 0.42 0.02 0.07 5.8 16.4 0.42 0.03 0.08 7.0 19.8 0.01 0.03 2.7 7.7 2.7 7.6 181 182 197 0.28 0.02 0.07 8.7 24.6 0.28 0.03 0.07 9.4 26.7 0.01 0.03 4.2 12.0 4.3 12.1 183 184 204 0.71 0.04 0.12 5.9 16.7 0.72 0.04 0.12 6.0 17.0 0.01 0.04 2.1 5.9 2.1 5.9 185 186 205 0.42 0.03 0.07 6.3 17.8 0.42 0.03 0.07 6.2 17.6 0.01 0.03 2.8 8.0 2.8 8.0Back to Top DSR COMPLEX SHEAR MODULUS AT 60C, G* (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 169 170 128 2.23 0.17 0.49 7.7 21.7 2.22 0.17 0.49 7.8 22.0 0.09 0.25 4.0 11.3 4.0 11.3Back to Top DSR PHASE ANGLE AT 60C, DELTA (DEGREES) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 169 170 120 85.7 0.6 1.6 0.7 1.8 85.7 0.6 1.7 0.7 2.0 0.4 1.0 0.4 1.2 0.4 1.2Back to Top DSR PHASE ANGLE AT 60C, DELTA (DEGREES) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 169 170 120 85.7 0.6 1.6 0.7 1.8 85.7 0.6 1.7 0.7 2.0 0.4 1.0 0.4 1.2 0.4 1.2Back to Top DSR G*/SIN DELTA AT 60C (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 169 170 131 2.24 0.17 0.49 7.7 21.9 2.23 0.18 0.50 8.0 22.5 0.09 0.25 4.0 11.3 4.0 11.3Back to Top DSR COMPLEX SHEAR MODULUS, G* (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 32 1.29 0.18 0.52 14.2 40.1 1.31 0.21 0.59 16.0 45.3 0.06 0.18 4.9 14.0 4.9 13.8 159 160 36 1.41 0.29 0.81 20.4 57.7 1.42 0.29 0.82 20.4 57.8 0.06 0.16 4.1 11.7 4.1 11.6 161 162 48 1.17 0.18 0.52 15.6 44.2 1.15 0.14 0.40 12.3 34.8 0.08 0.23 6.9 19.5 7.0 19.9 163 164 68 1.35 0.15 0.41 10.9 30.7 1.37 0.16 0.46 12.0 33.9 0.06 0.18 4.7 13.4 4.7 13.2 165 166 83 1.81 0.20 0.57 11.1 31.5 1.80 0.18 0.52 10.1 28.6 0.08 0.24 4.6 13.1 4.6 13.2 167 168 126 1.72 0.16 0.46 9.5 26.9 1.72 0.17 0.48 9.9 28.1 0.07 0.19 3.9 11.0 3.9 11.0 169 170 143 1.33 0.10 0.30 7.9 22.3 1.32 0.12 0.33 8.7 24.7 0.06 0.16 4.4 12.3 4.4 12.4 171 172 153 1.40 0.11 0.30 7.6 21.4 1.41 0.11 0.32 8.1 22.8 0.06 0.16 4.1 11.5 4.0 11.4 173 174 154 2.01 0.19 0.53 9.2 26.2 1.32 0.10 0.29 7.7 21.8 0.11 0.31 5.4 15.3 8.2 23.2 175 176 171 1.27 0.09 0.25 7.0 19.8 1.26 0.09 0.26 7.3 20.7 0.04 0.12 3.2 9.2 3.3 9.3 177 178 185 1.42 0.10 0.27 6.8 19.3 1.41 0.10 0.28 6.9 19.6 0.05 0.13 3.2 9.2 3.3 9.3 179 180 186 1.46 0.10 0.30 7.2 20.3 1.46 0.10 0.27 6.5 18.5 0.05 0.14 3.3 9.3 3.3 9.3 181 182 200 1.11 0.07 0.19 6.1 17.1 1.08 0.07 0.21 6.8 19.1 0.04 0.12 3.7 10.4 3.8 10.8 183 184 204 1.34 0.09 0.27 7.0 19.8 1.34 0.09 0.24 6.4 18.1 0.04 0.11 2.9 8.2 2.9 8.2 185 186 207 1.29 0.08 0.24 6.5 18.3 1.28 0.08 0.24 6.6 18.6 0.04 0.11 2.9 8.2 2.9 8.3Back to Top DSR PHASE ANGLE, DELTA (DEGREES) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 30 86.2 0.3 0.9 0.4 1.0 86.1 0.4 1.1 0.5 1.3 0.2 0.7 0.3 0.8 0.3 0.8 159 160 37 85.2 1.4 4.0 1.6 4.6 85.2 1.4 4.0 1.7 4.7 0.4 1.0 0.4 1.2 0.4 1.2 161 162 45 86.8 1.2 3.3 1.4 3.8 87.0 0.9 2.6 1.0 2.9 0.7 1.9 0.8 2.2 0.8 2.2 163 164 63 85.5 0.9 2.5 1.0 2.9 85.4 1.1 3.1 1.3 3.6 0.7 1.9 0.8 2.3 0.8 2.3 165 166 86 68.9 2.0 5.7 2.9 8.3 68.8 1.9 5.3 2.7 7.7 0.7 1.9 1.0 2.7 1.0 2.7 167 168 117 85.1 0.8 2.4 1.0 2.8 85.1 0.7 2.1 0.9 2.5 0.4 1.0 0.4 1.2 0.4 1.2 169 170 142 86.6 1.1 3.0 1.2 3.5 86.7 1.1 3.2 1.3 3.6 0.4 1.3 0.5 1.5 0.5 1.5 171 172 156 86.9 0.9 2.5 1.0 2.8 86.8 1.0 2.9 1.2 3.4 0.4 1.3 0.5 1.5 0.5 1.5 173 174 160 86.7 0.8 2.2 0.9 2.5 87.3 0.9 2.6 1.0 2.9 0.6 1.6 0.6 1.8 0.6 1.8 175 176 172 69.1 1.0 2.7 1.4 4.0 69.3 0.9 2.7 1.4 3.9 0.4 1.2 0.6 1.8 0.6 1.8 177 178 181 86.9 0.7 2.0 0.8 2.4 86.9 0.8 2.3 0.9 2.7 0.2 0.7 0.3 0.8 0.3 0.8 179 180 182 86.6 0.8 2.2 0.9 2.5 86.7 0.7 1.9 0.8 2.2 0.3 0.8 0.3 1.0 0.3 1.0 181 182 197 88.8 0.8 2.2 0.9 2.5 88.9 0.8 2.2 0.9 2.5 0.3 0.9 0.4 1.0 0.4 1.0 183 184 201 83.8 0.6 1.7 0.7 2.1 83.8 0.6 1.7 0.7 2.0 0.2 0.6 0.3 0.7 0.3 0.7 185 186 202 87.7 0.6 1.7 0.7 2.0 87.7 0.6 1.6 0.7 1.9 0.3 0.7 0.3 0.8 0.3 0.8Back to Top DSR G*/SIN DELTA (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 32 1.31 0.20 0.55 14.9 42.1 1.32 0.22 0.62 16.4 46.5 0.06 0.18 4.8 13.6 4.7 13.4 159 160 36 1.41 0.29 0.82 20.4 57.7 1.43 0.29 0.83 20.5 58.1 0.06 0.17 4.2 11.9 4.1 11.7 161 162 48 1.18 0.19 0.53 15.9 45.1 1.15 0.14 0.40 12.4 35.0 0.08 0.23 7.1 19.9 7.2 20.3 163 164 67 1.35 0.14 0.39 10.2 28.7 1.36 0.14 0.39 10.0 28.3 0.06 0.17 4.5 12.8 4.5 12.7 165 166 85 1.96 0.24 0.69 12.3 34.9 1.96 0.23 0.65 11.8 33.3 0.09 0.26 4.6 13.1 4.6 13.1 167 168 128 1.73 0.17 0.47 9.6 27.3 1.73 0.17 0.49 10.1 28.4 0.07 0.19 3.9 11.0 3.9 10.9 169 170 145 1.32 0.10 0.29 7.8 22.1 1.32 0.11 0.32 8.6 24.3 0.06 0.16 4.3 12.1 4.3 12.1 171 172 157 1.40 0.11 0.32 8.2 23.1 1.41 0.12 0.34 8.7 24.5 0.06 0.16 4.0 11.2 3.9 11.1 173 174 157 2.02 0.17 0.48 8.3 23.6 1.32 0.10 0.28 7.5 21.2 0.10 0.28 4.9 13.8 7.5 21.1 175 176 171 1.36 0.10 0.29 7.4 21.0 1.34 0.10 0.29 7.5 21.3 0.04 0.13 3.3 9.2 3.3 9.3 177 178 186 1.42 0.10 0.28 6.9 19.6 1.41 0.10 0.28 7.0 19.7 0.05 0.13 3.2 9.0 3.2 9.0 179 180 183 1.46 0.10 0.29 7.0 19.7 1.47 0.10 0.27 6.5 18.3 0.04 0.13 3.1 8.7 3.1 8.7 181 182 201 1.11 0.07 0.19 6.1 17.2 1.08 0.07 0.21 6.8 19.2 0.04 0.12 3.7 10.4 3.8 10.8 183 184 207 1.35 0.09 0.27 7.0 19.7 1.35 0.09 0.25 6.5 18.5 0.04 0.11 2.9 8.2 2.9 8.2 185 186 207 1.29 0.08 0.24 6.5 18.3 1.28 0.08 0.24 6.6 18.6 0.04 0.11 2.9 8.3 2.9 8.3Back to Top CHANGE IN MASS (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 32 0.001 0.05 0.15 -- -- -- 0.04 0.11 -- -- 0.030 0.086 -- -- -- -- 159 160 37 0.046 0.03 0.09 66 187 0.051 0.03 0.09 64 182 0.009 0.027 20 57 18 52 161 162 46 0.123 0.04 0.11 32 91 0.124 0.04 0.10 30 84 0.018 0.052 15 42 15 42 163 164 65 0.022 0.01 0.04 62 175 0.021 0.01 0.04 69 195 0.009 0.025 39 110 42 120 165 166 84 0.104 0.03 0.10 33 94 0.107 0.04 0.11 35 99 0.017 0.048 16 47 16 45 167 168 126 0.181 0.06 0.16 31 88 0.181 0.06 0.16 32 90 0.024 0.069 13 38 13 38 169 170 136 0.075 0.03 0.10 45 128 0.076 0.03 0.10 45 128 0.013 0.038 18 50 17 49 171 172 152 0.092 0.04 0.13 48 137 0.093 0.05 0.13 50 143 0.020 0.056 22 61 22 61 173 174 158 0.197 0.06 0.16 29 83 0.236 0.06 0.17 26 73 0.033 0.093 17 47 14 39 175 176 166 0.288 0.09 0.24 30 85 0.292 0.09 0.26 31 88 0.046 0.131 16 46 16 45 177 178 174 0.137 0.05 0.13 35 98 0.145 0.05 0.14 34 96 0.024 0.067 17 49 16 46 179 180 172 0.218 0.06 0.16 26 73 0.217 0.06 0.16 26 75 0.026 0.072 12 33 12 33 181 182 202 0.268 0.08 0.24 31 88 0.260 0.08 0.24 32 90 0.033 0.092 12 34 12 35 183 184 199 -0.063 0.05 0.13 -74 -211 -0.062 0.05 0.14 -80 -225 0.015 0.043 -24 -68 -24 -69 185 186 199 -0.255 0.07 0.21 -29 -82 -0.251 0.07 0.19 -26 -74 0.030 0.083 -12 -33 -12 -33Back to Top RTFO - DSR COMPLEX SHEAR MODULUS (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 32 2.93 0.42 1.18 14.3 40.4 2.97 0.35 1.00 11.9 33.6 0.15 0.43 5.2 14.7 5.1 14.5 159 160 37 3.63 0.79 2.24 21.8 61.6 3.56 0.82 2.31 22.9 64.7 0.24 0.66 6.5 18.3 6.6 18.7 161 162 47 2.64 0.32 0.91 12.2 34.6 2.59 0.35 1.00 13.6 38.5 0.18 0.51 6.9 19.5 7.0 19.9 163 164 66 3.23 0.44 1.25 13.6 38.5 3.27 0.39 1.09 11.8 33.4 0.20 0.56 6.1 17.3 6.0 17.1 165 166 84 3.05 0.40 1.13 13.2 37.2 3.08 0.39 1.10 12.6 35.6 0.16 0.44 5.2 14.6 5.1 14.5 167 168 126 4.01 0.46 1.31 11.5 32.6 3.97 0.47 1.32 11.7 33.2 0.16 0.45 4.0 11.3 4.0 11.4 169 170 138 2.85 0.27 0.77 9.6 27.1 2.85 0.29 0.81 10.1 28.5 0.15 0.43 5.3 15.0 5.3 15.0 171 172 151 3.07 0.27 0.75 8.7 24.5 3.05 0.28 0.80 9.2 26.1 0.12 0.35 4.0 11.3 4.0 11.4 173 174 152 4.09 0.39 1.11 9.6 27.2 2.61 0.25 0.71 9.6 27.3 0.22 0.62 5.3 15.1 8.4 23.7 175 176 170 2.54 0.22 0.62 8.7 24.5 2.55 0.24 0.68 9.5 26.8 0.13 0.36 5.0 14.1 5.0 14.1 177 178 183 3.19 0.28 0.79 8.7 24.7 3.18 0.27 0.78 8.6 24.4 0.15 0.43 4.8 13.5 4.8 13.6 179 180 181 3.19 0.27 0.77 8.6 24.3 3.20 0.28 0.78 8.6 24.3 0.11 0.31 3.4 9.7 3.4 9.6 181 182 198 2.38 0.21 0.59 8.7 24.7 2.29 0.21 0.58 9.0 25.4 0.09 0.26 3.9 11.0 4.1 11.5 183 184 203 2.62 0.27 0.77 10.4 29.5 2.63 0.26 0.73 9.8 27.8 0.12 0.34 4.6 13.1 4.6 13.1 185 186 204 3.06 0.26 0.73 8.4 23.9 3.07 0.27 0.77 8.9 25.1 0.14 0.40 4.7 13.2 4.7 13.2Back to Top RTFO - DSR PHASE ANGLE, DELTA (DEGREES) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 31 82.1 0.8 2.1 0.9 2.6 82.3 0.7 2.0 0.9 2.4 0.7 1.9 0.8 2.3 0.8 2.3 159 160 36 80.1 1.5 4.2 1.8 5.2 79.8 1.4 4.1 1.8 5.1 0.8 2.4 1.0 2.9 1.0 3.0 161 162 45 83.6 1.1 3.1 1.3 3.7 83.8 1.0 2.9 1.2 3.5 0.4 1.2 0.5 1.4 0.5 1.4 163 164 64 80.6 1.1 3.0 1.3 3.8 80.5 1.0 2.8 1.2 3.5 0.6 1.6 0.7 2.0 0.7 2.0 165 166 82 64.9 1.1 3.2 1.8 5.0 64.8 1.1 3.2 1.7 4.9 0.5 1.5 0.8 2.3 0.8 2.3 167 168 123 80.8 0.8 2.4 1.0 3.0 80.8 0.9 2.5 1.1 3.1 0.4 1.0 0.5 1.3 0.5 1.3 169 170 139 83.5 0.9 2.4 1.0 2.9 83.5 0.9 2.6 1.1 3.2 0.5 1.4 0.6 1.6 0.6 1.6 171 172 151 84.0 0.7 1.9 0.8 2.2 83.9 0.7 1.9 0.8 2.2 0.3 0.8 0.3 0.9 0.3 0.9 173 174 149 84.0 0.6 1.6 0.7 1.9 85.0 0.7 2.0 0.8 2.4 0.3 0.9 0.4 1.1 0.4 1.1 175 176 173 63.3 0.9 2.6 1.4 4.1 63.5 0.9 2.5 1.4 4.0 0.5 1.3 0.7 2.0 0.7 2.0 177 178 181 83.9 0.5 1.6 0.7 1.8 83.9 0.6 1.6 0.7 1.9 0.3 0.8 0.3 0.9 0.3 0.9 179 180 177 83.9 0.6 1.6 0.7 1.9 83.8 0.5 1.6 0.7 1.8 0.3 0.7 0.3 0.8 0.3 0.8 181 182 197 87.4 0.6 1.6 0.6 1.8 87.5 0.6 1.6 0.6 1.8 0.3 0.7 0.3 0.8 0.3 0.8 183 184 199 79.7 0.8 2.3 1.0 2.9 79.7 0.8 2.4 1.1 3.0 0.4 1.0 0.5 1.3 0.5 1.3 185 186 194 84.8 0.5 1.3 0.5 1.5 84.8 0.4 1.2 0.5 1.4 0.2 0.5 0.2 0.6 0.2 0.6Back to Top RTFO - DSR G*/SIN DELTA (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 32 2.96 0.43 1.20 14.4 40.7 2.99 0.37 1.03 12.2 34.6 0.15 0.43 5.1 14.5 5.1 14.3 159 160 37 3.69 0.82 2.32 22.2 62.8 3.62 0.84 2.38 23.2 65.7 0.24 0.68 6.5 18.5 6.7 18.8 161 162 47 2.65 0.33 0.93 12.3 34.9 2.60 0.35 1.00 13.6 38.5 0.18 0.52 6.9 19.6 7.1 20.0 163 164 68 3.30 0.46 1.30 13.9 39.4 3.34 0.41 1.16 12.3 34.7 0.20 0.57 6.1 17.4 6.1 17.1 165 166 86 3.38 0.47 1.33 13.9 39.3 3.40 0.45 1.27 13.2 37.2 0.18 0.50 5.2 14.8 5.2 14.8 167 168 127 4.06 0.46 1.30 11.3 32.0 4.03 0.46 1.30 11.4 32.2 0.16 0.46 4.0 11.3 4.0 11.4 169 170 140 2.87 0.27 0.78 9.6 27.1 2.87 0.29 0.82 10.1 28.6 0.15 0.43 5.2 14.8 5.2 14.8 171 172 154 3.08 0.28 0.79 9.0 25.6 3.06 0.29 0.81 9.4 26.5 0.12 0.35 4.0 11.4 4.0 11.4 173 174 157 4.12 0.40 1.13 9.7 27.6 2.62 0.24 0.69 9.3 26.4 0.22 0.63 5.4 15.2 8.5 23.9 175 176 172 2.85 0.27 0.76 9.4 26.7 2.86 0.30 0.85 10.5 29.7 0.15 0.41 5.1 14.4 5.1 14.4 177 178 185 3.21 0.28 0.80 8.9 25.1 3.20 0.28 0.78 8.6 24.4 0.15 0.43 4.8 13.5 4.8 13.6 179 180 181 3.21 0.27 0.77 8.4 23.9 3.21 0.28 0.79 8.7 24.7 0.13 0.37 4.1 11.6 4.1 11.5 181 182 197 2.38 0.21 0.60 8.9 25.1 2.29 0.21 0.58 9.0 25.3 0.11 0.30 4.4 12.5 4.6 13.0 183 184 203 2.66 0.28 0.79 10.5 29.6 2.68 0.27 0.76 10.0 28.3 0.13 0.36 4.8 13.6 4.8 13.5 185 186 204 3.07 0.26 0.74 8.5 24.0 3.08 0.28 0.78 9.0 25.4 0.15 0.42 4.8 13.6 4.8 13.6Back to Top PAV - DSR COMPLEX SHEAR MODULUS, G* (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 26 3308 530 1500 16.0 45.3 3309 595 1682 18.0 50.8 239 677 7.2 20.5 7.2 20.5 159 160 34 3062 723 2046 23.6 66.8 2947 748 2115 25.4 71.8 345 976 11.3 31.9 11.7 33.1 161 162 42 4510 1112 3146 24.7 69.7 4469 1078 3048 24.1 68.2 264 746 5.8 16.5 5.9 16.7 163 164 62 2909 886 2506 30.5 86.1 2877 878 2484 30.5 86.3 266 752 9.1 25.9 9.2 26.1 165 166 81 1674 348 984 20.8 58.8 1662 332 938 20.0 56.4 187 529 11.2 31.6 11.2 31.8 167 168 120 5920 1216 3439 20.5 58.1 5830 1223 3460 21.0 59.3 583 1649 9.8 27.9 10.0 28.3 169 170 132 4759 742 2100 15.6 44.1 4848 670 1894 13.8 39.1 318 901 6.7 18.9 6.6 18.6 171 172 144 3643 578 1635 15.9 44.9 3640 582 1648 16.0 45.3 224 635 6.2 17.4 6.2 17.4 173 174 151 6421 1209 3420 18.8 53.3 4292 839 2372 19.5 55.3 730 2064 11.4 32.1 17.0 48.1 175 176 172 1593 276 782 17.4 49.1 1598 266 753 16.7 47.1 128 361 8.0 22.7 8.0 22.6 177 178 175 4466 1016 2874 22.8 64.4 4465 1015 2871 22.7 64.3 328 927 7.3 20.8 7.3 20.8 179 180 176 3790 621 1757 16.4 46.3 3794 685 1937 18.1 51.1 233 659 6.1 17.4 6.1 17.4 181 182 196 5428 1053 2978 19.4 54.9 5360 1051 2974 19.6 55.5 360 1017 6.6 18.7 6.7 19.0 183 184 200 3066 595 1684 19.4 54.9 3073 604 1708 19.6 55.6 248 700 8.1 22.8 8.1 22.8 185 186 189 4943 841 2378 17.0 48.1 4906 827 2339 16.9 47.7 412 1166 8.3 23.6 8.4 23.8Back to Top PAV - DSR PHASE ANGLE, DELTA (DEGREES) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 27 47.7 1.5 4.3 3.2 9.0 47.7 1.3 3.7 2.7 7.7 0.7 1.8 1.4 3.9 1.4 3.9 159 160 33 47.2 2.0 5.5 4.1 11.7 47.2 1.4 4.1 3.1 8.7 1.0 2.9 2.2 6.2 2.2 6.2 161 162 42 48.1 1.8 5.2 3.8 10.9 48.2 2.0 5.6 4.1 11.5 0.7 2.0 1.5 4.1 1.4 4.1 163 164 60 47.6 2.0 5.7 4.2 11.9 47.6 1.8 5.0 3.7 10.4 0.8 2.3 1.7 4.9 1.7 4.9 165 166 84 51.6 1.5 4.3 2.9 8.3 51.6 1.3 3.7 2.5 7.1 0.6 1.7 1.2 3.3 1.2 3.3 167 168 114 46.9 1.2 3.4 2.6 7.2 46.8 1.2 3.4 2.6 7.3 0.6 1.6 1.2 3.4 1.2 3.4 169 170 132 49.7 1.2 3.3 2.3 6.6 49.7 1.1 3.2 2.3 6.4 0.4 1.1 0.8 2.3 0.8 2.3 171 172 142 49.8 1.2 3.3 2.3 6.5 49.7 1.1 3.2 2.3 6.5 0.5 1.5 1.1 3.0 1.1 3.0 173 174 150 51.9 1.2 3.4 2.3 6.5 54.8 1.2 3.5 2.2 6.4 0.8 2.3 1.5 4.3 1.5 4.1 175 176 169 50.6 1.3 3.6 2.5 7.1 50.5 1.2 3.4 2.4 6.7 0.7 1.9 1.3 3.8 1.3 3.8 177 178 169 49.2 2.0 5.8 4.2 11.8 49.1 1.9 5.4 3.9 11.0 0.6 1.7 1.2 3.4 1.2 3.4 179 180 172 53.1 1.0 2.8 1.9 5.3 53.1 1.1 3.1 2.1 5.8 0.5 1.3 0.9 2.5 0.9 2.5 181 182 191 56.1 1.6 4.5 2.8 8.0 56.2 1.6 4.6 2.9 8.2 0.7 1.9 1.2 3.4 1.2 3.4 183 184 197 49.5 1.4 4.1 2.9 8.2 49.5 1.5 4.1 3.0 8.4 0.6 1.8 1.3 3.6 1.3 3.6 185 186 197 50.2 1.3 3.6 2.5 7.1 50.3 1.2 3.3 2.3 6.5 0.5 1.4 1.0 2.8 1.0 2.8Back to Top PAV - DSR G*SIN DELTA (KPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 26 2431 365 1033 15.0 42.5 2442 430 1216 17.6 49.8 168 475 6.9 19.6 6.9 19.5 159 160 34 2246 482 1363 21.5 60.7 2149 512 1448 23.8 67.4 233 659 10.4 29.3 10.8 30.6 161 162 41 3322 667 1887 20.1 56.8 3285 609 1722 18.5 52.4 191 541 5.8 16.3 5.8 16.5 163 164 60 2253 504 1425 22.4 63.2 2237 477 1349 21.3 60.3 200 565 8.9 25.1 8.9 25.3 165 166 83 1282 280 792 21.9 61.8 1278 263 745 20.6 58.2 144 406 11.2 31.7 11.2 31.8 167 168 120 4310 830 2349 19.3 54.5 4292 839 2372 19.5 55.3 367 1039 8.5 24.1 8.6 24.2 169 170 137 3625 564 1595 15.6 44.0 3646 548 1549 15.0 42.5 285 807 7.9 22.2 7.8 22.1 171 172 141 2787 367 1037 13.2 37.2 2786 351 994 12.6 35.7 162 458 5.8 16.5 5.8 16.5 173 174 153 5117 839 2373 16.4 46.4 3529 629 1779 17.8 50.4 535 1512 10.4 29.6 15.2 42.9 175 176 168 1224 180 509 14.7 41.6 1226 181 512 14.8 41.8 94 267 7.7 21.8 7.7 21.7 177 178 176 3389 734 2075 21.7 61.2 3387 755 2134 22.3 63.0 253 717 7.5 21.1 7.5 21.2 179 180 177 3044 487 1376 16.0 45.2 3047 537 1518 17.6 49.8 187 529 6.1 17.4 6.1 17.4 181 182 198 4523 843 2384 18.6 52.7 4463 846 2392 19.0 53.6 288 815 6.4 18.0 6.5 18.3 183 184 198 2344 411 1164 17.6 49.6 2364 433 1225 18.3 51.8 163 462 7.0 19.7 6.9 19.5 185 186 192 3820 593 1677 15.5 43.9 3799 585 1653 15.4 43.5 299 844 7.8 22.1 7.9 22.2Back to Top BBR CREEP STIFFNESS (MPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 24 125 13 37 10.4 29.5 127 13 38 10.5 29.8 5 15 4.4 12.3 4.3 12.2 159 160 34 179 15 44 8.6 24.3 185 15 43 8.2 23.3 8 22 4.2 12.0 4.1 11.6 161 162 39 291 38 107 13.0 36.7 292 36 101 12.2 34.6 14 41 4.9 14.0 4.9 13.9 163 164 55 183 21 58 11.3 32.0 183 20 56 10.8 30.6 8 22 4.3 12.1 4.3 12.1 165 166 78 128 10 27 7.6 21.4 128 9 25 6.8 19.2 5 13 3.7 10.4 3.7 10.4 167 168 111 336 32 91 9.6 27.1 334 29 83 8.8 24.9 14 41 4.3 12.1 4.3 12.2 169 170 128 309 34 96 10.9 30.9 311 34 95 10.8 30.6 12 34 3.9 11.0 3.9 10.9 171 172 140 187 16 46 8.7 24.7 188 16 47 8.7 24.7 8 24 4.5 12.7 4.5 12.6 173 174 154 391 45 127 11.5 32.5 299 30 86 10.2 28.7 25 71 6.4 18.2 8.4 23.7 175 176 172 221 23 66 10.6 29.9 220 22 63 10.1 28.7 10 28 4.4 12.5 4.5 12.6 177 178 177 284 25 71 8.9 25.1 283 27 75 9.4 26.5 12 33 4.1 11.5 4.1 11.6 179 180 174 183 15 42 8.1 22.9 184 14 40 7.6 21.5 6 18 3.4 9.6 3.4 9.6 181 182 196 180 19 54 10.6 30.0 177 19 54 10.7 30.3 9 25 4.8 13.6 4.9 13.9 183 184 201 179 14 40 7.9 22.3 179 14 38 7.6 21.5 5 14 2.8 7.9 2.8 7.8 185 186 198 196 14 40 7.3 20.6 197 14 41 7.3 20.8 7 20 3.6 10.1 3.6 10.1Back to Top BBR SLOPE (m) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 27 0.348 0.013 0.038 3.9 11.0 0.346 0.015 0.042 4.3 12.1 0.005 0.016 1.6 4.5 1.6 4.5 159 160 36 0.340 0.014 0.039 4.0 11.4 0.340 0.014 0.039 4.1 11.5 0.004 0.012 1.2 3.5 1.2 3.5 161 162 40 0.298 0.016 0.044 5.3 14.9 0.301 0.016 0.044 5.2 14.7 0.008 0.021 2.5 7.1 2.5 7.1 163 164 59 0.344 0.018 0.051 5.3 14.9 0.343 0.017 0.049 5.1 14.4 0.007 0.020 2.1 5.9 2.1 5.9 165 166 82 0.358 0.016 0.045 4.5 12.7 0.357 0.016 0.046 4.6 12.9 0.008 0.021 2.1 5.9 2.1 6.0 167 168 113 0.297 0.014 0.040 4.8 13.6 0.297 0.015 0.041 4.9 14.0 0.007 0.019 2.3 6.6 2.3 6.6 169 170 128 0.309 0.013 0.036 4.2 11.8 0.308 0.013 0.036 4.1 11.6 0.006 0.017 1.9 5.4 1.9 5.4 171 172 145 0.331 0.012 0.035 3.8 10.6 0.330 0.012 0.033 3.5 9.9 0.005 0.015 1.6 4.5 1.6 4.5 173 174 152 0.305 0.013 0.038 4.4 12.5 0.337 0.012 0.035 3.7 10.5 0.008 0.024 2.8 7.8 2.5 7.0 175 176 167 0.322 0.012 0.034 3.7 10.6 0.323 0.012 0.034 3.7 10.5 0.005 0.015 1.7 4.7 1.7 4.7 177 178 177 0.306 0.012 0.034 3.9 11.1 0.306 0.013 0.036 4.1 11.7 0.005 0.014 1.6 4.4 1.6 4.4 179 180 176 0.358 0.009 0.025 2.5 7.1 0.358 0.009 0.024 2.4 6.8 0.004 0.012 1.2 3.4 1.2 3.4 181 182 191 0.369 0.012 0.033 3.2 8.9 0.370 0.012 0.033 3.2 9.0 0.005 0.014 1.4 3.8 1.4 3.8 183 184 196 0.334 0.009 0.025 2.6 7.3 0.334 0.009 0.026 2.8 7.9 0.005 0.014 1.5 4.2 1.5 4.2 185 186 198 0.330 0.010 0.029 3.1 8.8 0.330 0.010 0.030 3.2 9.0 0.005 0.014 1.5 4.2 1.5 4.2Back to Top DT FAILURE STRESS (MPa) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 10 1.75 0.74 2.09 42 119 1.90 0.79 2.23 41 117 0.22 0.62 13 35 12 33 159 160 8 1.95 0.83 2.35 43 121 1.80 0.73 2.08 41 115 0.20 0.56 10 29 11 31 161 162 4 1.68 0.23 0.65 14 39 2.00 0.43 1.21 22 61 0.19 0.53 11 31 9 26 163 164 7 1.95 0.59 1.68 30 86 1.98 0.75 2.12 38 107 0.12 0.33 6 17 6 17 165 166 9 1.83 0.70 1.98 38 108 1.71 0.53 1.50 31 88 0.25 0.70 14 38 15 41 167 168 7 2.03 0.99 2.79 49 137 2.19 0.81 2.29 37 105 0.27 0.77 13 38 12 35 169 170 9 3.32 1.13 3.19 34 96 2.90 1.30 3.67 45 127 0.41 1.17 12 35 14 40 171 172 9 3.05 0.89 2.53 29 83 3.00 0.95 2.67 32 89 0.41 1.16 13 38 14 39 173 174 9 3.72 1.52 4.31 41 116 3.60 1.47 4.16 41 116 0.54 1.52 14 41 15 42 175 176 14 3.41 1.56 4.41 46 129 3.45 1.51 4.28 44 124 0.22 0.63 7 19 6 18 177 178 18 3.68 1.18 3.33 32 90 3.70 1.22 3.45 33 93 0.43 1.21 12 33 12 33 179 180 32 4.02 0.86 2.44 21 61 4.05 0.99 2.81 25 70 0.32 0.90 8 22 8 22 181 182 39 2.73 0.59 1.67 22 61 2.80 0.60 1.70 22 61 0.29 0.81 11 30 10 29 183 184 46 3.87 0.87 2.45 22 63 3.96 0.77 2.17 19 55 0.36 1.01 9 26 9 26 185 186 51 3.71 0.59 1.68 16 45 3.78 0.63 1.78 17 47 0.27 0.76 7 21 7 20Back to Top DT FAILURE STRAIN (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SMPL 2ND SMPL 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 155 156 10 1.25 0.43 1.21 34 97 1.32 0.46 1.31 35 99 0.29 0.81 23 65 22 61 159 160 8 1.43 1.68 4.76 117 332 1.34 1.63 4.60 121 343 0.13 0.38 9 26 10 28 161 162 4 0.65 0.55 1.55 84 239 0.50 0.58 1.63 116 327 0.15 0.42 23 64 30 84 163 164 7 0.73 0.61 1.72 83 235 0.81 0.96 2.72 118 334 0.26 0.74 36 101 32 91 165 166 9 1.25 0.85 2.40 68 192 1.03 0.61 1.73 60 169 0.38 1.08 30 86 37 105 167 168 7 0.58 0.41 1.17 72 203 0.64 0.41 1.15 64 180 0.08 0.21 13 37 12 34 169 170 9 1.13 0.66 1.87 59 166 1.02 0.70 1.99 69 194 0.15 0.41 13 37 14 40 171 172 10 1.68 0.66 1.86 39 111 1.62 0.64 1.81 40 112 0.27 0.78 16 46 17 48 173 174 10 0.73 0.25 0.71 35 98 1.00 0.42 1.20 42 120 0.21 0.61 30 84 21 61 175 176 14 1.51 1.02 2.89 68 191 1.63 1.23 3.47 75 213 0.38 1.07 25 71 23 66 177 178 19 0.94 0.34 0.96 36 102 0.99 0.29 0.83 30 84 0.17 0.47 18 50 17 48 179 180 31 1.91 0.47 1.34 25 70 1.91 0.56 1.60 30 84 0.36 1.01 19 53 19 53 181 182 38 0.93 0.28 0.80 30 85 0.96 0.27 0.77 28 79 0.14 0.39 15 42 14 40 183 184 45 1.82 0.65 1.83 36 101 1.87 0.72 2.03 38 109 0.28 0.78 15 43 15 42 185 186 53 1.38 0.34 0.97 25 71 1.45 0.37 1.03 25 71 0.17 0.48 12 35 12 33Back to Top |