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SECTION IIIc.
SPECIFIC GRAVITY, 60/60F, METHOD T227 KINEMATIC VISCOSITY AT 60C (CENTISTOKE) FLASH POINT, TAG OPEN CUP (DEG F) FLASH POINT, TAG OPEN CUP (DEG C) VOLUME OF DISTILLATE AT NOMINAL 225C (PERCENT) VOLUME OF DISTILLATE AT NOMINAL 260C (PERCENT) VOLUME OF DISTILLATE AT NOMINAL 316C (PERCENT) TOTAL DISTILLATE AT NOMINAL 360C (PERCENT OF TOTAL SAMPLE) PENETRATION OF THE RESIDUE (0.1 MM) KINEMATIC VISCOSITY OF THE RESIDUE AT 135C (CENTISTOKE) VISCOSITY OF THE RESIDUE AT 60C (POISE) SOLUBILITY OF THE RESIDUE IN TRICHLOROETHYLENE (PERCENT) SAYBOLT FUROL VISCOSITY AT 140C (SECOND) SPECIFIC GRAVITY, 60/60F, METHOD T227 MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 31 32 71 0.9649 0.0027 0.0064 0.28 0.78 0.9702 0.0037 0.0076 0.38 1.09 0.0017 0.0049 0.18 0.51 0.18 0.51Back to Top KINEMATIC VISCOSITY AT 60C (CENTISTOKE) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 49 280.7 11.0 31.3 3.9 11.2 499.0 18.0 49.6 3.5 9.9 12.1 34.2 4.3 12.2 2.4 6.9 * 9 10 48 310.2 7.8 22.0 2.5 7.1 375.1 8.4 23.6 2.2 6.3 4.6 13.1 1.5 4.2 1.2 3.5 11 12 50 35.2 0.85 2.4 2.4 6.8 56.4 1.79 5.1 3.2 9.0 1.00 2.82 2.8 8.0 1.8 5.0 * 13 14 60 289.4 14.0 39.8 4.9 13.8 516.6 19.0 53.3 3.7 10.3 9.3 26.3 3.2 9.1 1.8 5.1 * 31 32 83 303.9 7.2 20.4 2.4 6.7 442.7 12.4 35.2 2.8 8.0 7.3 20.6 2.4 6.8 1.6 4.7 * 37 38 88 297.1 9.3 26.2 3.1 8.8 416.5 10.5 29.7 2.5 7.1 6.9 19.5 2.3 6.6 1.7 4.7 43 44 82 470.1 7.8 22.1 1.7 4.7 322.8 9.6 27.2 3.0 8.4 6.7 19.0 1.4 4.0 2.1 5.9 * 49 50 89 332.3 12.0 33.3 3.5 10.0 373.8 13.0 37.6 3.6 10.1 10.6 30.0 3.2 9.0 2.8 8.0 55 56 87 295.8 9.9 28.0 3.4 9.5 389.6 13.3 37.5 3.4 9.7 8.2 23.2 2.8 7.8 2.1 6.0 * 61 62 89 398.9 13.0 37.6 3.3 9.4 333.8 11.0 30.3 3.2 9.1 8.4 23.8 2.1 6.0 2.5 7.1 * 67 68 90 278.7 8.4 23.9 3.0 8.6 362.6 17.3 48.8 4.8 13.5 11.9 33.8 4.3 12.1 3.3 9.3 * 73 74 93 115.8 4.1 11.5 3.5 9.9 115.9 3.8 10.8 3.3 9.3 1.7 4.7 1.4 4.1 1.4 4.1 79 80 102 307.9 15.0 42.7 4.9 13.9 337.4 13.0 36.0 3.8 10.7 8.8 24.9 2.9 8.1 2.6 7.4 * 85 86 96 1025.0 37.0 104.2 3.6 10.2 1032.1 34.0 97.3 3.3 9.4 23.0 65.0 2.2 6.3 2.2 6.3 91 92 98 456.4 13.0 35.8 2.8 7.9 456.7 14.0 39.4 3.1 8.6 9.5 26.8 2.1 5.9 2.1 5.9 97 98 90 477.6 17.0 46.8 3.5 9.8 478.8 12.0 33.3 2.5 7.0 10.9 30.8 2.3 6.4 2.3 6.4 * 103 104 85 488.4 12.0 32.9 2.4 6.7 486.4 13.0 37.7 2.7 7.8 7.8 22.0 1.6 4.5 1.6 4.5 109 110 87 965.2 33.8 95.6 3.5 9.9 956.1 31.6 89.5 3.3 9.4 20.2 57.0 2.1 5.9 2.1 6.0 115 116 87 37.3 0.9 2.6 2.5 7.0 36.7 0.8 2.3 2.3 6.4 0.5 1.3 1.2 3.4 1.2 3.5 121 122 88 172.8 5.1 14.5 3.0 8.4 167.4 4.4 12.5 2.6 7.5 3.2 9.2 1.9 5.3 1.9 5.5 127 128 92 310.5 11.0 31.1 3.5 10.0 316.1 12.1 34.1 3.8 10.8 7.3 20.5 2.3 6.6 2.3 6.5 133 134 86 393.8 13.1 37.1 3.3 9.4 393.0 13.4 38.0 3.4 9.7 7.9 22.4 2.0 5.7 2.0 5.7 139 140 93 454.5 12.4 35.2 2.7 7.7 452.7 12.5 35.3 2.8 7.8 8.6 24.4 1.9 5.4 1.9 5.4 145 146 88 452.9 13.9 39.4 3.1 8.7 457.1 13.5 38.2 3.0 8.4 9.3 26.2 2.0 5.8 2.0 5.7 151 152 79 711.4 45.5 128.8 6.4 18.1 594.3 44.3 125.4 7.5 21.1 38.2 108.1 5.4 15.2 6.4 18.2Back to Top FLASH POINT, TAG OPEN CUP (DEG F) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 48 133.1 10 28.4 7.5 21.3 135.4 11 31.7 8.3 23.4 7.8 22.2 5.9 16.7 5.8 16.4 9 10 42 187.1 12 33.1 6.3 17.7 190.1 12 34.8 6.5 18.3 5.2 14.7 2.8 7.9 2.7 7.7 11 12 53 160.7 13 35.4 7.8 22.0 161.3 11 32.3 7.1 20.0 6.2 17.5 3.8 10.9 3.8 10.8 13 14 61 105.2 11 32.3 10.8 30.6 121.6 14 39.4 11.5 32.5 7.4 20.9 7.0 19.9 6.1 17.2 31 32 82 182.0 11 31.2 6.1 17.1 187.7 12 32.9 6.2 17.5 5.3 14.9 2.9 8.2 2.8 7.9 37 38 79 181.3 10 29.3 5.7 16.2 186.2 12 33.9 6.5 18.3 6.2 17.6 3.4 9.7 3.3 9.5 43 44 78 193.4 9.2 26.1 4.8 13.5 186.8 11.2 31.7 6.0 17.0 6.6 18.8 3.4 9.7 3.6 10.1 * 49 50 78 190.9 9.8 27.7 5.1 14.5 187.4 9.4 26.5 5.0 14.2 5.9 16.8 3.1 8.8 3.2 9.0 Back to Top FLASH POINT, TAG OPEN CUP (DEG C) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 55 56 60 75.2 6.9 19.5 9.2 26.0 88.7 11.4 32.3 12.9 36.5 7.9 22.3 10.5 29.7 8.9 25.1 * 61 62 73 82.8 6.7 18.8 8.0 22.8 80.3 6.6 18.7 8.2 23.3 3.4 9.6 4.1 11.6 4.2 11.9 67 68 64 87.6 5.2 14.8 6.0 17.0 90.0 5.5 15.4 6.1 17.1 2.7 7.6 3.1 8.7 3.0 8.4 73 74 76 72.6 7.7 21.7 10.6 29.9 72.5 7.3 20.5 10.0 28.3 3.2 9.0 4.4 12.4 4.4 12.4 79 80 84 90.3 7.0 19.9 7.8 22.1 89.9 8.0 22.7 8.9 25.2 2.6 7.3 2.9 8.1 2.9 8.2 85 86 69 92.8 7.3 20.6 7.9 22.2 92.6 7.8 22.2 8.5 24.0 4.0 11.3 4.3 12.2 4.3 12.2 91 92 79 84.3 7.6 21.6 9.1 25.7 84.5 8.0 22.6 9.5 26.8 2.8 8.0 3.3 9.4 3.3 9.4 97 98 74 80.5 7.3 20.6 9.1 25.6 80.7 7.5 21.2 9.3 26.3 2.6 7.4 3.2 9.1 3.2 9.1 103 104 72 81.3 6.6 18.8 8.2 23.1 80.0 7.6 21.5 9.5 26.9 2.9 8.2 3.6 10.1 3.6 10.3 109 110 63 90.1 8.6 24.5 9.6 27.1 89.6 6.8 19.2 7.6 21.4 3.5 10.0 3.9 11.1 3.9 11.2 * 115 116 76 84.3 5.4 15.3 6.4 18.1 83.7 5.3 14.9 6.3 17.8 2.3 6.4 2.7 7.6 2.7 7.6 121 122 73 77.0 6.4 18.2 8.4 23.7 77.6 6.3 17.7 8.1 22.8 3.2 9.0 4.1 11.7 4.1 11.6 127 128 77 84.6 6.2 17.5 7.3 20.7 84.6 6.3 17.9 7.5 21.2 2.0 5.8 2.4 6.8 2.4 6.8 133 134 75 47.2 7.5 21.2 15.9 44.9 46.9 7.3 20.8 15.6 44.3 1.7 4.8 3.6 10.2 3.6 10.2 139 140 80 83.2 6.8 19.2 8.2 23.1 83.1 6.8 19.2 8.2 23.1 1.9 5.4 2.3 6.4 2.3 6.4 145 146 69 83.0 5.8 16.4 7.0 19.8 83.1 5.7 16.2 6.9 19.5 2.3 6.5 2.8 7.9 2.8 7.9 151 152 59 92.2 5.7 16.0 6.1 17.4 90.6 5.8 16.5 6.5 18.3 3.4 9.7 3.7 10.6 3.8 10.8Back to Top VOLUME OF DISTILLATE AT NOMINAL 225C (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 59 33.8 1.6 4.6 4.8 13.6 45.1 1.8 5.1 4.0 11.4 1.4 3.9 4.1 11.6 3.1 8.7 11 12 57 13.7 2.2 6.2 16 45 10.3 2.3 6.5 22 63 1.5 4.3 11 31 15 42 13 14 68 66.8 1.5 4.2 2.2 6.2 61.4 2.6 7.4 4.3 12.1 1.9 5.5 2.9 8.2 3.1 8.9 * 37 38 92 3.2 2.0 85.0 62 175 2.8 2.1 0.6 49 139 17.7 50.0 -- -- -- -- * 55 56 85 10.9 3.3 9.3 30 86 0.1 0.6 1.7 -- -- 2.4 6.7 22 61 -- -- * 61 62 87 3.9 2.5 7.1 65 184 4.8 2.4 6.9 51 143 1.7 4.7 43 122 35 98 67 68 82 0.5 1.0 2.7 199 563 0.3 0.6 1.7 218 617 0.5 1.5 111 315 198 559 * 73 74 93 11.1 6.4 18.1 58 163 10.8 6.4 18.1 59 168 3.6 10.2 32 92 33 94 85 86 95 0.4 1.9 5.3 -- -- 0.2 0.7 1.9 -- -- 1.3 3.7 -- -- -- -- * 91 92 93 3.1 2.6 7.4 86 242 3.1 2.8 7.9 90 254 1.0 3.0 34 97 34 96 97 98 93 7.6 3.0 8.6 40 114 8.0 3.1 8.7 39 109 1.5 4.3 20 57 19 54 103 104 84 4.2 3.4 9.5 80 226 4.9 3.4 9.6 69 196 1.2 3.5 29 83 25 71 109 110 87 0.4 1.4 3.9 370 1047 0.4 1.7 4.9 440 1245 0.4 1.2 112 317 108 305 115 116 81 0.4 0.9 2.4 199 562 0.4 0.7 2.1 175 495 0.3 0.8 67 190 69 195 121 122 90 10.9 3.3 9.3 30 86 8.7 3.0 8.4 34 97 1.7 4.9 16 45 20 57 127 128 84 0.7 1.2 3.3 177 501 0.8 1.3 3.7 168 474 0.7 1.8 100 283 83 236 133 134 84 54.0 4.3 12.3 8 23 53.1 4.4 12.4 8 23 2.0 5.6 4 10 4 11 139 140 95 2.8 2.7 7.6 97 274 2.8 2.6 7.3 92 259 1.0 2.8 35 99 34 97 145 146 91 4.9 2.9 8.1 59 167 3.7 2.5 7.0 66 187 1.0 2.9 21 59 27 77 151 152 82 19.0 7.7 21.8 41 115 9.0 4.7 13.3 52 148 4.7 13.3 25 70 52 148Back to Top VOLUME OF DISTILLATE AT NOMINAL 260C (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 60 51.1 1.7 4.8 3.3 9.4 62.4 1.5 4.3 2.4 6.8 1.1 3.0 2.1 5.9 1.7 4.8 9 10 59 31.8 2.4 6.8 7.6 21.5 30.1 2.5 7.2 8.4 23.9 2.0 5.5 6.1 17.4 6.5 18.4 11 12 57 54.6 1.7 4.9 3.2 9.0 51.6 2.4 6.7 4.6 12.9 1.2 3.3 2.1 6.1 2.3 6.4 * 13 14 68 82.0 1.1 3.2 1.4 3.9 78.6 2.6 7.3 3.3 9.3 1.8 5.2 2.2 6.3 2.3 6.6 * 31 32 83 39.4 2.1 6.0 5.4 15.2 34.5 2.2 6.1 6.2 17.6 1.6 4.5 4.0 11.4 4.6 13.0 37 38 89 26.5 3.2 9.1 12.2 34.5 23.4 2.9 8.2 12.4 35.1 2.2 6.3 8.4 23.7 9.5 26.8 43 44 87 23.9 2.1 6.0 8.8 24.9 30.4 2.2 6.2 7.2 20.4 1.5 4.3 6.3 17.8 4.9 14.0 49 50 88 22.8 2.5 7.2 11.1 31.4 26.0 2.3 6.6 9.0 25.4 1.3 3.8 5.9 16.6 5.1 14.6 55 56 85 52.1 2.9 8.2 5.6 15.8 28.1 3.5 9.9 12.4 35.0 2.3 6.7 4.5 12.8 8.4 23.7 61 62 87 30.6 3.5 10.0 11.5 32.6 32.7 3.2 9.1 9.8 27.8 2.3 6.6 7.6 21.5 7.1 20.1 67 68 83 30.6 3.2 8.9 10.3 29.1 27.7 2.8 7.9 10.0 28.3 1.9 5.5 6.3 17.9 7.0 19.7 73 74 92 54.2 4.6 13.0 8.5 23.9 53.7 4.9 13.9 9.2 25.9 2.8 7.9 5.1 14.5 5.2 14.7 79 80 100 41.9 2.9 8.1 6.8 19.3 41.2 2.9 8.1 6.9 19.6 1.7 4.8 4.0 11.5 4.1 11.6 85 86 96 27.1 3.4 9.6 12.5 35.4 27.3 3.4 9.6 12.4 35.1 1.3 3.6 4.6 13.1 4.6 13.0 91 92 96 32.9 4.1 11.6 12.5 35.4 32.8 3.5 9.8 10.6 30.0 2.4 6.8 7.3 20.7 7.4 20.8 97 98 92 43.4 2.4 6.8 5.6 15.8 43.5 2.5 7.0 5.7 16.0 1.4 3.9 3.2 9.1 3.2 9.1 103 104 82 46.7 2.8 8.0 6.1 17.2 47.8 2.3 6.4 4.7 13.4 1.8 5.1 3.8 10.8 3.7 10.6 109 110 89 28.9 3.1 8.7 10.6 30.0 28.4 3.7 10.3 12.9 36.3 1.9 5.4 6.6 18.7 6.7 19.1 115 116 85 57.2 2.5 7.1 4.4 12.4 57.3 2.3 6.5 4.0 11.3 1.2 3.4 2.1 5.9 2.1 5.9 121 122 88 61.6 1.9 5.4 3.1 8.8 60.8 2.0 5.6 3.3 9.3 1.3 3.7 2.1 6.0 2.1 6.1 127 128 90 34.2 3.9 10.9 11.3 32.0 34.4 2.8 7.9 8.1 23.0 2.3 6.5 6.7 19.0 6.7 18.8 133 134 84 74.6 2.4 6.8 3.2 9.1 74.1 2.3 6.6 3.1 8.9 1.3 3.6 1.7 4.8 1.7 4.9 139 140 93 36.8 3.4 9.5 9.1 25.8 36.1 3.1 8.6 8.5 23.9 2.2 6.1 5.9 16.6 6.0 16.9 145 146 88 36.9 2.3 6.5 6.2 17.6 37.9 2.2 6.3 5.9 16.7 1.6 4.4 4.2 11.9 4.1 11.6 151 152 77 33.9 5.9 16.6 17.3 49.0 32.8 3.8 10.7 11.5 32.6 3.2 9.0 9.4 26.6 9.7 27.5Back to Top VOLUME OF DISTILLATE AT NOMINAL 316C (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 60 76.8 1.5 4.2 2.0 5.5 82.2 1.7 4.8 2.1 5.9 1.2 3.5 1.6 4.5 1.5 4.2 9 10 61 79.9 1.8 5.1 2.3 6.4 78.6 1.7 4.8 2.2 6.2 1.2 3.5 1.6 4.4 1.6 4.5 11 12 58 86.7 0.9 2.5 1.0 2.8 85.1 1.4 4.0 1.7 4.7 0.8 2.3 0.9 2.6 0.9 2.6 * 13 14 67 93.0 1.6 4.6 1.7 4.9 91.8 2.4 6.9 2.7 7.5 2.0 5.6 2.1 6.0 2.1 6.1 * 31 32 83 80.7 1.4 3.9 1.7 4.8 78.0 1.4 3.9 1.8 5.0 1.0 2.9 1.3 3.6 1.3 3.7 37 38 89 74.3 1.6 4.5 2.2 6.1 72.5 1.9 5.4 2.7 7.5 1.3 3.7 1.8 5.0 1.8 5.1 * 43 44 87 73.8 1.7 4.9 2.4 6.7 77.6 1.4 3.9 1.8 5.0 1.3 3.6 1.7 4.9 1.7 4.7 * 49 50 86 74.0 1.5 4.3 2.1 5.8 74.0 1.6 4.7 2.2 6.3 1.2 3.5 1.7 4.7 1.7 4.7 55 56 88 85.2 1.3 3.7 1.5 4.3 79.2 2.6 7.3 3.3 9.2 1.8 5.2 2.1 6.1 2.3 6.5 * 61 62 85 77.6 1.7 4.9 2.2 6.3 78.6 1.7 4.9 2.2 6.3 1.3 3.6 1.6 4.7 1.6 4.6 67 68 84 80.6 1.7 4.8 2.1 5.9 78.7 2.1 5.8 2.6 7.4 1.3 3.8 1.6 4.7 1.7 4.8 * 73 74 90 86.3 1.4 3.9 1.6 4.6 86.3 1.4 3.9 1.6 4.6 0.8 2.4 1.0 2.8 1.0 2.8 79 80 100 84.4 1.5 4.2 1.8 5.0 84.3 1.4 3.9 1.6 4.6 1.0 2.8 1.2 3.3 1.2 3.3 85 86 96 79.2 1.7 4.7 2.1 6.0 79.5 2.0 5.7 2.5 7.1 1.1 3.1 1.4 4.0 1.4 3.9 * 91 92 95 77.4 1.9 5.3 2.4 6.8 77.6 2.0 5.6 2.5 7.2 0.9 2.6 1.2 3.4 1.2 3.4 97 98 89 80.6 1.8 5.0 2.2 6.2 80.3 2.0 5.7 2.5 7.0 1.1 3.1 1.4 3.8 1.4 3.8 103 104 83 81.5 1.7 4.8 2.1 5.9 82.1 1.7 4.9 2.1 6.0 1.0 3.0 1.3 3.6 1.3 3.6 109 110 85 78.2 1.5 4.4 2.0 5.6 78.4 1.7 4.9 2.2 6.3 1.3 3.7 1.7 4.8 1.7 4.8 115 116 87 90.1 0.9 2.5 1.0 2.8 90.1 0.9 2.4 1.0 2.7 0.7 1.9 0.7 2.1 0.7 2.1 121 122 90 89.4 1.5 4.2 1.7 4.7 89.5 1.2 3.4 1.3 3.8 1.0 2.9 1.1 3.2 1.1 3.2 * 127 128 89 79.4 1.9 5.5 2.4 6.9 79.3 1.6 4.4 2.0 5.6 1.0 2.8 1.2 3.5 1.2 3.5 133 134 86 90.8 1.5 4.2 1.6 4.6 90.8 1.6 4.6 1.8 5.1 0.9 2.7 1.0 3.0 1.0 3.0 139 140 91 78.4 2.1 5.9 2.6 7.5 78.5 1.7 4.7 2.1 6.0 1.0 2.9 1.3 3.7 1.3 3.7 145 146 82 78.7 1.6 4.5 2.0 5.8 78.8 1.4 3.9 1.8 5.0 1.0 2.9 1.3 3.7 1.3 3.7 151 152 75 78.2 2.6 7.3 3.3 9.3 77.8 2.5 7.1 3.2 9.1 1.7 4.9 2.2 6.3 2.2 6.3Back to Top TOTAL DISTILLATE AT NOMINAL 360C (PERCENT OF TOTAL SAMPLE) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 58 25.8 0.89 2.52 3.5 9.8 21.9 0.76 2.14 3.5 9.8 0.43 1.21 1.7 4.7 2.0 5.5 9 10 59 23.5 0.61 1.72 2.6 7.3 22.1 0.62 1.76 2.8 8.0 0.45 1.26 1.9 5.4 2.0 5.7 11 12 54 46.3 1.00 2.82 2.2 6.1 41.7 1.07 3.01 2.6 7.2 0.71 2.00 1.5 4.3 1.7 4.8 13 14 60 25.5 0.67 1.90 2.6 7.4 22.0 0.82 2.33 3.7 10.6 0.60 1.69 2.3 6.6 2.7 7.7 31 32 84 26.4 0.67 1.90 2.5 7.2 24.0 0.60 1.70 2.5 7.1 0.40 1.14 1.5 4.3 1.7 4.8 37 38 89 28.3 0.64 1.81 2.3 6.4 26.0 0.56 1.58 2.2 6.1 0.34 0.96 1.2 3.4 1.3 3.7 43 44 88 25.0 0.71 2.01 2.9 8.1 27.7 0.72 2.03 2.6 7.3 0.40 1.12 1.6 4.5 1.4 4.0 49 50 90 27.3 0.80 2.27 3.0 8.3 26.7 0.78 2.20 2.9 8.3 0.41 1.15 1.5 4.2 1.5 4.3 55 56 87 25.2 0.70 1.99 2.8 7.9 23.2 0.68 1.91 2.9 8.2 0.43 1.22 1.7 4.8 1.9 5.3 61 62 84 23.9 0.54 1.54 2.3 6.4 25.3 0.63 1.79 2.5 7.1 0.36 1.01 1.5 4.2 1.4 4.0 67 68 81 26.4 0.56 1.58 2.1 6.0 24.4 0.66 1.85 2.7 7.6 0.35 1.00 1.3 3.8 1.4 4.1 73 74 91 33.2 0.95 2.69 2.9 8.1 33.4 0.87 2.47 2.6 7.4 0.45 1.26 1.3 3.8 1.3 3.8 79 80 103 25.8 1.02 2.88 4.0 11.2 25.1 0.81 2.30 3.2 9.2 0.54 1.54 2.1 6.0 2.2 6.1 * 85 86 97 18.6 0.59 1.67 3.2 9.0 18.6 0.59 1.66 3.2 8.9 0.25 0.72 1.4 3.9 1.4 3.9 91 92 95 23.9 0.69 1.94 2.9 8.2 23.8 0.66 1.87 2.8 7.8 0.29 0.83 1.2 3.5 1.2 3.5 97 98 93 22.0 0.65 1.85 3.0 8.4 22.1 0.77 2.17 3.5 9.8 0.35 0.99 1.6 4.5 1.6 4.5 103 104 82 22.7 0.63 1.78 2.8 7.8 22.9 0.60 1.70 2.6 7.4 0.37 1.06 1.6 4.7 1.6 4.6 109 110 87 18.6 0.55 1.55 2.9 8.3 18.6 0.48 1.35 2.6 7.3 0.34 0.95 1.8 5.1 1.8 5.1 115 116 89 44.9 1.26 3.55 2.8 7.9 45.2 1.55 4.39 3.4 9.7 0.49 1.40 1.1 3.1 1.1 3.1 * 121 122 89 31.8 0.87 2.45 2.7 7.7 32.2 0.77 2.17 2.4 6.7 0.34 0.95 1.1 3.0 1.0 3.0 127 128 89 22.8 0.73 2.06 3.2 9.0 22.8 0.66 1.88 2.9 8.3 0.28 0.80 1.2 3.5 1.2 3.5 133 134 87 24.2 0.62 1.77 2.6 7.3 24.2 0.64 1.80 2.6 7.4 0.27 0.77 1.1 3.2 1.1 3.2 139 140 96 21.4 0.69 1.94 3.2 9.1 21.5 0.70 1.98 3.3 9.2 0.32 0.91 1.5 4.2 1.5 4.2 145 146 88 22.5 0.68 1.93 3.0 8.6 22.5 0.58 1.64 2.6 7.3 0.29 0.83 1.3 3.7 1.3 3.7 151 152 80 22.2 1.23 3.48 5.6 15.7 21.9 0.79 2.23 3.6 10.2 0.69 1.94 3.1 8.8 3.1 8.9Back to Top PENETRATION OF THE RESIDUE (0.1 MM) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 59 172.4 18 52 11 30 143.5 17 49 12 34 10.7 30.2 6.2 17.5 7.4 21.0 9 10 59 185.8 15 43 8 23 184.8 15 43 8 23 8.0 22.5 4.3 12.1 4.3 12.2 11 12 62 201.4 32 92 16 46 190.4 26 74 14 38 13.7 38.9 6.8 19.3 7.2 20.4 * 13 14 65 92.5 6 16 6 17 91.2 4 11 4 12 2.7 7.7 2.9 8.3 3.0 8.4 * 31 32 85 192.7 20 56 10 29 205.0 19 55 10 27 10.1 28.6 5.2 14.8 4.9 14.0 37 38 91 182.6 21 59 12 33 173.6 19 53 11 30 8.1 23.0 4.5 12.6 4.7 13.2 43 44 87 175.7 20 57 11 32 183.3 23 64 12 35 13.1 37.0 7.4 21.1 7.1 20.2 49 50 89 205.6 23 64 11 31 209.1 26 73 12 35 14.4 40.8 7.0 19.8 6.9 19.5 55 56 84 195.6 25 72 13 37 267.5 27 76 10 28 23.6 66.9 12.1 34.2 8.8 25.0 61 62 84 151.7 20 58 14 38 152.2 20 57 13 38 13.3 37.6 8.8 24.8 8.7 24.7 67 68 83 139.9 23 64 16 46 137.0 22 63 16 46 10.7 30.3 7.7 21.7 7.8 22.1 73 74 77 260.5 30 84 11 32 260.1 29 83 11 32 10.4 29.3 4.0 11.2 4.0 11.3 79 80 101 185.1 26 74 14 40 185.5 25 72 14 38 12.2 34.5 6.6 18.6 6.6 18.6 85 86 97 176.2 19 53 11 30 177.5 20 58 12 33 10.4 29.4 5.9 16.7 5.9 16.6 91 92 96 205.7 29 82 14 40 206.4 31 87 15 42 12.1 34.2 5.9 16.6 5.9 16.6 97 98 93 210.8 24 67 11 32 209.0 22 63 11 30 9.2 26.1 4.4 12.4 4.4 12.5 103 104 81 171.3 21 60 12 35 170.0 21 59 12 35 10.0 28.4 5.9 16.6 5.9 16.7 109 110 89 159.1 16 45 10 28 157.3 16 45 10 29 8.9 25.2 5.6 15.9 5.7 16.1 115 116 83 175.6 33 93 19 53 174.2 29 82 17 47 14.8 41.9 8.4 23.9 8.5 24.1 121 122 88 113.1 16 45 14 40 112.5 15 43 13 38 6.8 19.3 6.0 17.1 6.1 17.2 127 128 89 145.6 14 41 10 28 147.0 15 41 10 28 6.2 17.5 4.3 12.0 4.2 11.9 133 134 86 108.1 12 33 11 30 109.1 11 31 10 28 4.6 13.1 4.3 12.1 4.2 12.0 139 140 94 224.1 28 80 13 36 225.3 29 83 13 37 11.9 33.6 5.3 15.0 5.3 14.9 145 146 87 197.1 32 91 16 46 197.6 31 89 16 45 14.2 40.2 7.2 20.4 7.2 20.4 151 152 76 137.7 21 59 15 43 129.9 19 53 14 41 9.8 27.6 7.1 20.0 7.5 21.2Back to Top KINEMATIC VISCOSITY OF THE RESIDUE AT 135C (CENTISTOKE) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 31 32 81 233.2 14 41 6 17 234.6 15 43 6 18 8.6 24.4 3.7 10.5 3.7 10.4 37 38 83 299.0 24 67 8 22 313.1 22 62 7 20 9.9 28.0 3.3 9.4 3.2 8.9 43 44 81 322.7 25 70 8 22 312.8 29 82 9 26 14.5 41.1 4.5 12.7 4.6 13.1 49 50 85 275.5 24 68 9 25 274.2 27 75 10 27 14.2 40.3 5.2 14.6 5.2 14.7 55 56 81 255.7 23 66 9 26 207.4 15 43 7 21 14.9 42.3 5.8 16.5 7.2 20.4 * 61 62 76 288.6 27 77 9 27 289.9 23 65 8 22 18.7 52.8 6.5 18.3 6.4 18.2 67 68 74 301.4 24 69 8 23 306.0 21 59 7 19 16.2 45.8 5.4 15.2 5.3 15.0 73 74 80 176.6 13 35 7 20 178.0 12 33 7 19 7.5 21.1 4.2 11.9 4.2 11.9 79 80 92 187.8 14 39 7 21 187.9 14 41 8 22 7.2 20.5 3.9 10.9 3.9 10.9 85 86 85 248.9 16 45 6 18 249.3 17 48 7 19 10.4 29.4 4.2 11.8 4.2 11.8 91 92 87 250.9 24 69 10 27 253.6 25 70 10 28 11.3 32.0 4.5 12.8 4.5 12.6 97 98 90 227.7 17 49 8 21 229.9 16 44 7 19 9.5 26.9 4.2 11.8 4.1 11.7 103 104 81 273.3 24 69 9 25 278.2 26 72 9 26 14.3 40.5 5.2 14.8 5.1 14.6 109 110 83 256.3 17 49 7 19 258.0 17 48 7 19 7.4 20.9 2.9 8.2 2.9 8.1 115 116 84 244.9 33 92 13 38 248.9 29 83 12 33 11.2 31.5 4.6 12.9 4.5 12.7 121 122 84 319.8 32 91 10 28 321.1 29 82 9 26 13.3 37.7 4.2 11.8 4.2 11.8 127 128 88 158.1 12 34 8 22 157.6 11 31 7 20 5.5 15.5 3.5 9.8 3.5 9.8 133 134 84 339.0 25 70 7 21 341.6 24 68 7 20 10.8 30.4 3.2 9.0 3.1 8.9 139 140 90 210.1 20 58 10 27 211.2 21 58 10 28 8.6 24.2 4.1 11.5 4.1 11.5 145 146 84 236.5 24 69 10 29 237.6 22 63 9 26 11.7 33.0 4.9 14.0 4.9 13.9 151 152 78 272.1 27 76 10 28 286.4 32 90 11 31 16.0 45.2 5.9 16.6 5.6 15.8Back to Top VISCOSITY OF THE RESIDUE AT 60C (POISE) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 31 32 71 556 72 205 13 37 545 73 206 13 38 46 130 8 23 8 24 37 38 78 813 122 346 15 42 895 111 313 12 35 55 157 7 19 6 18 43 44 82 887 184 522 21 59 855 173 489 20 57 82 233 9 26 10 27 49 50 82 685 103 292 15 43 680 115 325 17 48 53 151 8 22 8 22 55 56 81 615 104 295 17 48 382 44 123 11 32 72 205 12 33 19 54 * 61 62 82 809 142 402 18 50 818 114 323 14 40 88 249 11 31 11 30 * 67 68 80 878 148 420 17 48 913 140 396 15 43 86 244 10 28 9 27 73 74 85 306 44 123 14 40 309 43 122 14 40 19 53 6 17 6 17 79 80 98 413 63 179 15 43 410 61 173 15 42 32 90 8 22 8 22 85 86 92 608 86 243 14 40 612 77 218 13 36 47 133 8 22 8 22 91 92 91 605 114 323 19 53 603 109 308 18 51 47 134 8 22 8 22 97 98 90 535 86 244 16 46 549 91 257 17 47 44 124 8 23 8 23 103 104 84 740 143 404 19 55 766 139 392 18 51 62 175 8 24 8 23 109 110 84 743 95 268 13 36 755 93 264 12 35 46 130 6 18 6 17 115 116 87 560 139 393 25 70 576 133 375 23 65 53 150 9 27 9 26 121 122 92 1175 251 710 21 60 1175 245 694 21 59 97 276 8 23 8 23 127 128 88 592 83 236 14 40 588 87 247 15 42 23 64 4 11 4 11 133 134 85 1350 212 600 16 44 1348 187 530 14 39 77 219 6 16 6 16 139 140 95 456 101 285 22 63 458 98 276 21 60 30 86 7 19 7 19 145 146 88 582 130 367 22 63 582 126 356 22 61 57 160 10 28 10 28 151 152 80 840 205 579 24 69 909 271 768 30 84 112 318 13 38 12 35Back to Top SOLUBILITY OF THE RESIDUE IN TRICHLOROETHYLENE (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 58 99.883 0.11 0.29 0.11 0.32 99.880 0.10 0.29 0.10 0.29 -- -- -- -- -- -- * 9 10 57 99.850 0.11 0.29 0.11 0.32 99.880 0.10 0.29 0.10 0.29 -- -- -- -- -- -- * 9 10 57 99.851 0.11 0.32 0.11 0.32 99.857 0.12 0.34 0.12 0.34 0.05 0.14 0.05 0.14 0.05 0.14 11 12 60 99.817 0.15 0.41 0.15 0.42 99.800 0.15 0.43 0.15 0.43 0.05 0.13 0.05 0.13 0.05 0.13 13 14 68 99.853 0.12 0.34 0.12 0.34 99.853 0.12 0.34 0.12 0.35 -- -- -- -- -- -- *Back to Top SAYBOLT FUROL VISCOSITY AT 140C (SECOND) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE OPERATOR PRECISION SAMPLE NO. 1st SMPL 2nd SMPL 1st SMPL 2nd SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 52 138.7 7.1 20.1 5.1 14.5 248.5 14.8 41.9 6.0 16.9 -- -- -- -- -- -- * 9 10 51 151.4 6.2 17.5 4.1 11.5 182.9 6.4 18.1 3.5 9.9 3.25 9.21 2.15 6.08 1.78 5.04 11 12 52 20.4 0.7 1.8 3.2 9.1 28.8 1.5 4.3 5.3 15.0 -- -- -- -- -- -- * 13 14 55 147.4 11.1 31.4 7.5 21.3 257.0 16.4 46.3 6.4 18.0 -- -- -- -- -- -- * 31 32 79 150.5 8.8 24.9 5.8 16.5 216.9 12.0 34.0 5.5 15.7 -- -- -- -- -- -- * 37 38 68 144.6 5.7 5.7 4.0 11.2 202.1 7.5 7.5 3.7 10.5 -- -- -- -- -- -- * 43 44 70 232.2 13.7 38.6 5.9 16.6 157.5 7.8 22.2 5.0 14.1 11.77 33.32 5.07 14.35 7.48 21.16Back to Top |